Bulletin of the Korean Chemical Society

Korean Chemical Society (대한화학회)
권호 표지
DOI QR코드

DOI QR Code

Direct Chiral Separation of N-Fluorenylmethoxycarbonyl α-Amino Acids by HPLC for Determination of Enantiomeric Purity

  • Published : 2005.06.20
Download PDF
⟨ Previous Next ⟩

Abstract

Keywords

References

  1. Greene, T. W.; Wuts, P. G. M. Protective Groups in Organic Synthesis, 3rd Ed.; John Wiley & Sons. Inc.: New York, 1999
  2. Einarsson, S.; Folestad, S.; Josefsson, B.; Lagerkvist, S. Anal. Chem. 1986, 58, 1638 https://doi.org/10.1021/ac00121a010
  3. Bruckner, H.; Lupke, M. J. Chromatogr. A 1996, 697, 295 https://doi.org/10.1016/0021-9673(94)00938-6
  4. Burgess, K. Solid-Phase Organic Synthesis, 3rd Ed.; John Wiley & Sons. Inc.: New York, 2000
  5. Jung, G. Combinatorial Chemistry: Synthesis, Analysis, Screening; Wiley-VCH: Tubingen, 1999
  6. Zukowski, J.; Pawlowska, M.; Armstrong, D. W. J. Chromatogr. 1992, 623, 33 https://doi.org/10.1016/0021-9673(92)85295-5
  7. Tang, Y.; Zukowski, J.; Armstrong, D. W. J. Chromatogr. A 1996, 743, 261 https://doi.org/10.1016/0021-9673(96)00302-0
  8. Ekborg-Ott, K. H.; Liu, Y.; Armstrong, D. W. Chirality 1998, 10, 434 https://doi.org/10.1002/(SICI)1520-636X(1998)10:5<434::AID-CHIR10>3.0.CO;2-0
  9. Piccinini, A.-M.; Schmid, M. G.; Pajpanova, T.; Pancheva, S.; Grueva, E.; Gubitz, G. J. Biochem. Biophys. Methods 2004, 61, 11 https://doi.org/10.1016/j.jbbm.2004.02.004
  10. Oi, H.; Kitahara, H.; Aoki, F.; Kisu, N. J. Chromatogr. A 1995, 689, 195 https://doi.org/10.1016/0021-9673(94)00890-L
  11. Pirkle, W. H.; Lee, W. Bull. Korean Chem. Soc. 1998, 19, 1277
  12. Krawinkler, K. H.; Maier, N. M.; Sajovic, E.; Lindner, W. J. Chromatogr. A 2004, 1053, 119 https://doi.org/10.1016/j.chroma.2004.07.046
  13. Knoche, B.; Milosavljev, S.; Gropper, S.; Brunner, L. A.; Powell, M. L. J. Chromatogr. B 1997, 695, 355 https://doi.org/10.1016/S0378-4347(97)00196-5
  14. Application guide for chiral HPLC selection, third Edition, Daicel Chemical Industries, Ltd
  15. Kim, B.-H.; Lee, W. J. Liq. Chromatogr. & Rel. Tech. 1999, 22, 523 https://doi.org/10.1081/JLC-100101677
  16. Lee, W.; Kim, B.-H. J. High Resol. Chromatogr. 1998, 21, 189 https://doi.org/10.1002/(SICI)1521-4168(19980301)21:3<189::AID-JHRC189>3.0.CO;2-3
  17. Bodansky, M.; Bodansky, A. The Practice of Peptide Synthesis; Springer: New York, 1984
  18. Perry, J. A.; Rateike, J. D.; Szczerba, T. J. J. Chromatogr. 1987, 389, 57 https://doi.org/10.1016/S0021-9673(01)94410-3

Cited by

  1. -histidine-derived poly (ionic liquid)/silica nanocomposites and their application in the enantioselective hydrolysis of a chiral ester vol.131, pp.1, 2013, https://doi.org/10.1002/app.39595
  2. -PADs) of natural and unnatural amino acids: an analytical strategy for the key starting materials of therapeutic peptides vol.10, pp.21, 2018, https://doi.org/10.1039/C8AY00502H
  3. Comparative Liquid Chromatographic Enantiomer Resolution on Two Chiral Stationary Phases Derived from Amylose Tris(3,5-dimethylphenylcarbamate) vol.26, pp.7, 2005, https://doi.org/10.5012/bkcs.2005.26.7.1132
  4. Chiral Separation of N-Fluorenylmethoxycarbonyl α -Amino Acids on Quinine Carbamate-Bonded Silica by High Performance Liquid Chromatography vol.29, pp.1, 2005, https://doi.org/10.5012/bkcs.2008.29.1.257
  5. Enantiomer Separation of N-Protected α -Amino Acids on Covalently Immobilized Cellulose Tris(3,5-chlorophenylcarbamate) Chiral Stationary Phase in HPLC vol.29, pp.2, 2008, https://doi.org/10.5012/bkcs.2008.29.2.491
  6. Enantioseparation of N-fluorenylmethoxycarbonyl α-amino acids on polysaccharide-derived chiral stationary phases by reverse mode liquid chromatography vol.46, pp.5, 2005, https://doi.org/10.1016/j.jpba.2008.01.012
  7. Synthesis of Enantiopure γ-Glutamic Acid Functionalized Peptide Nucleic Acid Monomers vol.31, pp.7, 2010, https://doi.org/10.5012/bkcs.2010.31.7.2054
  8. 고성능 액체 크로마토그래피에서 아미노산과 이들 에스테르의 플루오레닐메톡시카르보닐 유도체의 자외선과 형광 검출에서의 동시 광학분리 vol.30, pp.4, 2005, https://doi.org/10.7841/ksbbj.2015.30.4.197
  9. Determination of Chemical and Enantiomeric Purity of α‐Amino Acids and their Methyl Esters as N‐Fluorenylmethoxycarbonyl Derivatives Using Amylose‐derived Chiral Stationary vol.40, pp.4, 2005, https://doi.org/10.1002/bkcs.11694