대한약전 (KPVIII) 수재 생약의 지표성분 정량법

Analytical Method for the Determination of Standard Compounds in Oriental Medicine Materials Listed in the Korean Pharmacopoeia (KPVIII)

  • Kim Kwan-Su (Dept. of Medicinal Plant Res., College of Nat. Sci., Mokpo Nat'l Univ.) ;
  • Kim Hocheol (Dept. of Herbal Pharmacology, College of Oriental Medicine, Kyung Hee Univ.)
  • 발행 : 2004.10.01

초록

키워드

참고문헌

  1. Asano, T., C. Sadakane, K. Ishihara, T. Yanagisawa, M. Kimura, and H. Kamei. 2001. Highperformance liquid chromatographic assay with fluorescence detection for the determination of cephaeline and emetine in human plasma and urine. J. of Chromatography B: Biomedical Sciences and Applications 757(2): 197-206 https://doi.org/10.1016/S0378-4347(01)00170-0
  2. Baricevic, D., A. Umek, S. Kreft, B. Maticic, and A. Zupancic. 1999. Effect of water stress and nitrogen fertilization on the content of hyoscyamine and scopolamine in the roots of deadly nightshade (Atropa belladonna). Environmental and Experimental Botany 42(1): 17-24 https://doi.org/10.1016/S0098-8472(99)00014-3
  3. Belajova, E. and M. Suhaj. 2004. Determination of phenolic constituents in citrus juices: Method of high performance liquid chromatography. Food Chemistry 86(3): 339-343 https://doi.org/10.1016/j.foodchem.2003.09.037
  4. Berenguer-Navarro, v., R. M. Giner-Galvan, N. Grane-Teruel, and G. Arrazola-Paternina. 2002. Chromatographic determination of cyanoglycosides prunasin and amygdalin in plant extracts using a porous graphitic carbon column. J. Agric. Food & Chern. 50(24): 6960-6963 https://doi.org/10.1021/jf0256081
  5. Bessieres, M. A., Y. Gilbon, J. C. Lefeuvre, and F. Larher. 1999. A single-step purification for glycine betaine determination in plant extracts by isocratic HPLC. J. Agric. Food & Chern. 47(9): 3718-3722 https://doi.org/10.1021/jf990031h
  6. Chen, F., H. T. Lu, and Y. Jiang. 2004. Purification of paeoniflorin from Paeonia lactiflora Pall. by high-speed counter-current chromatography. J. of Chromatography A 1040(2): 205-208 https://doi.org/10.1016/j.chroma.2004.04.023
  7. Choi, Y. H., Y. M. Sohn, C. Y. Kim, K. Y. Oh, and J. W. Kim. 2004. Analysis of strychnine from detoxified Strychno nux-vomica seeds using liquid chromatography-electrospray mass spectrometry. J. of Ethnopharmacology 93(1): 109-112 https://doi.org/10.1016/j.jep.2004.03.038
  8. Choi, Y. H., Y. W. Chin, J. W. Kim, S. H. Jeon, and K. P. Yoo. 1999. Strategies for supercritical fluid extraction of hyoscyamine and scopolamine salts using basified modifiers. J. of Chromatography A 863(1): 47-55 https://doi.org/10.1016/S0021-9673(99)00962-0
  9. Dost, K., and G. Davidson. 2000. Development of a packed-column supercritical fluid chromatography/atmospheric pressure chemical-ionisation mass spectrometric technique for the analysis of atropine. J. Biochem. Biophys. Methods 43(1-3): 125-134 https://doi.org/10.1016/S0165-022X(00)00055-5
  10. Ebata, N., K. Nakajima, K. Hayashi, M. Okada, and M. Maruno. 1996. Saponins from the root of Bupleurum falcatum. Phytochemistry 41(3): 895-901 https://doi.org/10.1016/0031-9422(95)00720-2
  11. Eldawy, M. A., M. M. Mabrouk, and F. A. El-Barbary. 2003. Determination of chlorpheniramine maleate and tincture ipecac in dosage form by liquid chromatography with ultraviolet detection. J. AOAC Int. 86(4): 675-680
  12. Frank, S. and Jr. Santamour. 1998. Amygdalin in Prunus leaves. Phytochemistry 47(8): 1537-1538 https://doi.org/10.1016/S0031-9422(97)00787-5
  13. Frederich, M., Y. H. Choi, and R. Verpoorte. 2003. Quantitative analysis of strychnine and brucine in Strychnos nux-vomica using IH-NMR. Planta Med. 69(12): 1169-1171 https://doi.org/10.1055/s-2003-818014
  14. Hazra, B., M. D. Sarma, and U. Sanyal. 2004. Separation methods of quinonoid constituents of plants used in oriental traditional medicines. J. of Chromatography B. in press
  15. He, X. G., M. W. Bernart, L. Z. Lian, and L. Z. Lin. 1998. High-performance liquid chromatography· electrospray mass spectrometric analysis of pungent constituents of ginger. J. of Chromatography A 796(2): 327-334 https://doi.org/10.1016/S0021-9673(97)01013-3
  16. Jiang, Y, H. T. Lu, and E Chen. 2004. Preparative purification of glycyrrhizin extracted from the root of liquorice using high-speed counter-current chromatography. J. of Chromatography A 1033(1): 183-186 https://doi.org/10.1016/j.chroma.2004.01.033
  17. Kim, J. S., H. Tanaka, and Y Shoyama. 2004. Immunoquantitative analysis for berberine and its related compounds using monoclonal antibodies in herbal medicines. Analyst. 129(1): 87-91 https://doi.org/10.1039/b311304c
  18. Li, H., B. Li, Y. Jiang, and F. Chen. 2004. Separation methods used for Scutellaria baicalensis active components. J. of Chromatography B. in press
  19. Mouly, P., E. M. Gaydou, and A. Auffray. 1998. Simultaneous separation of flavanone glycosides and polymethoxylated f1avones in citrus juices using liquid chromatography. J of Chromatogrphy A 800(2): 171-179 https://doi.org/10.1016/S0021-9673(97)01131-X
  20. Nogata, Y., H. Ohta, K. I. Yoza, M. Berhow, and S. Hasegawa. 1994. High-performance liquid chromatographic determination of naturally occurring f1avonoids in Citrus with a photodiode-array detector. J. of Chromatography A 667(1-2): 59-66 https://doi.org/10.1016/0021-9673(94)89051-X
  21. Phadke, M., R. T. Sane, S. N. Menon, P. S. Hijli, M. Shah, and P. H. Patel. 1998. Accelerated stability study on gingerol from Zingiber officinale using high performance thin layer chromatographic method. Toxicology Letters 95(S 1): 152
  22. Roman, M. C. 2004. Determination of ephedrine alkaloids in botanicals and dietary supplements by HPLC-UV: collaborative study. J. AOAC Int. 87(1): 1-14
  23. Schaneberg, B. T., S. Crockett, E. Bedir, and I. A. Khan. 2003. The role of chemical fingerprinting:application to Ephedra. Phytochemistry 62(6): 911-918 https://doi.org/10.1016/S0031-9422(02)00716-1
  24. Sun, S. W. and H. T. Su. 2002. Validated HPLC method for determination of sennosides A and B in senna tablets. J. Pharm. Biomed. Anal. 29(5): 881-894 https://doi.org/10.1016/S0731-7085(02)00208-X
  25. Takei, H., K. Nakauchi, and F. Yoshizaki. 2001. Analysis of swertiamarin in Swertia herb and preparations containing this crude drug by capillary electrophoresis. Anal. Sci. 17(7): 885-888 https://doi.org/10.2116/analsci.17.885
  26. Tsai, T. H. and C. F. Chen. 1992. Identification and determination of honokiol and magnolol from Magnolia officinalis by high-performance liquid chromatography with phtodiode-array UV detection. J. of Chromatography A 598(1): 143-146 https://doi.org/10.1016/0021-9673(92)85125-D
  27. Wang, X., Y. Wang, Y. Geng, ELi, and C. Zheng. 2004. Isolation and purification of honokiol and magnolol from cortex Magnolia officinalis by high-speed counter-current chromatography. J. of Chromatography A 1036(2): 171-175 https://doi.org/10.1016/j.chroma.2004.02.073
  28. Xu, H., A. C. Templeton, and R. A. Reed. 2003. Quantification of 5-HMF and dextrose in commercial aqueous dextrose solutions. J. Pharm. Biomed. Anal. 32(3): 451-459 https://doi.org/10.1016/S0731-7085(03)00163-8
  29. Xu, Y. C., L. X. Wei, and Y. L. Wang. 2001. Determination of cinnamic acid in Cinnamomum cassia Presl after compatibility in Coptis chinensis Franch. Zhongguo Zhong Yao Za Zhi 26(1): 47-49
  30. Yang, E, T. Zhang, R. Zhang, and Y. Ito. 1998. Application of analytical and preparative high-speed counter-current chromatography for separation of alkaloids from Coptis chinensis Franch. J. of Chromatography A 829(1-2): 137-141 https://doi.org/10.1016/S0021-9673(98)00776-6
  31. Yu, B. S., X. P. Yan, G. B. Zhen, and Y. P. Rao. 2002. RP-HPLC determination of puerarin in Chinese traditional medicinal preparations containing pueraria. J. Pharm. Biomed. Anal. 30: 843-849 https://doi.org/10.1016/S0731-7085(02)00326-6
  32. Zhang, Q., A. Myint, L. Liu, X. Ge, and H. Cui. 2004. Flow injection-chemiluminescence determination of puerarin in pharmaceutical preparations. J. of Pharm. Biomed. Anal. in press
  33. Zhao, S., Q. Liu, X.Chen, and Z. Hu. 2004. Separation and determination of gentiopicroside and swertiamarin in Tibetan medicines by micellar electrokinetic electrophoresis. Biomed. Chromatogr. 18(1) : 10-5 https://doi.org/10.1002/bmc.285
  34. Zhu, S. H., S. Shimokawa, H. Tanaka, and Y. Shoyama. 2004. Development of an assay system for saikosaponin a using anti-saikosaponin a monoclonal antibodies. BioI. Pharm. Bull. 27(1): 66-71 https://doi.org/10.1248/bpb.27.66
  35. 강신복, 조정희, 김혜수, 김영림, 오미현, 강인호, 심영훈, 지선경, 함일권, 원도희, 김영중. 1997. 생약제제의 약제학적 연구(XI): 건강 및 그 함유제제의 성분추출량에 관한 연구. 식품의약품안전본부 연보 1: 236-241
  36. 김호철. 2001. 한약약리학. 집문당
  37. 명노홍, 채영주, 김명희. 1999. 모세관전기영동장치 및 고속액체 크로마토그래피에 의한 황금의 성분 분석법 비교 연구. 서울특별시보건환경연구원. 보건환경연구논문집 34: 42-50
  38. 명노홍, 채영주, 이강문. 2000. 모세관전기영동장치 및 고속액체 크로마토그래피에 의한 목단피의 성분 분석법 비교 연구. 서울특별시보건환경연구원. 보건환경연구논문집 36: 39-45
  39. 식품의약품안전청 대한약전제8개정편찬위원회. 2002. 대한약전 제8개정. (주)약업신문
  40. 식품의약품안전청. 2002. 대한약전외한약(생약)규격집. 동원문화사
  41. 원도희, 조정희, 김혜수, 고정현, 이종필, 박상애, 이하정, 육창수, 김일혁, 원봉필. 1997. 생약 및 생약제제의 규격에 관한 연구(XIV) -산수유의 분석법. 식품의약품안전본부연보 1: 197-201
  42. 원도희. 1991. 상용생약의 성분정량. 성은
  43. 일본약국방해설서편집위원회. 2001. 제14개정 일본약국방해설서. 광천서점
  44. 강승엽, 강신정, 이종필, 박상용, 신지현, 정영자, 박진영, 하광원, 박종희, 박정일. 1998. 계피, 계지 및 계심의 규격 및 품질평가법에 관한 연구. 식품의약품안전청연보 2: 223-232
  45. 정명근. 2002. 작약 식물체 부위별 성분 함량 변이. 한국약용작물학회지 10(5): 392-398
  46. 조정희, 강신복, 김혜수, 김영림, 오미현, 강인호, 박성수, 심영훈, 지선경, 함일권, 하광원, 김영중, 박만기. 1998. 생약의 표준화에 관한 연구(IV); 후박, 창출 및 백출의 표준화에 관한 연구. 식품의 약품안전청연보 2: 238-252
  47. 조정희, 강신복, 김혜수, 김영림, 오미현, 강인호, 박성수, 지선경, 함일권, 박만기. 1997. 생약표준화에 관한 연구(III) -글리시리진산 표준품 규격에 관한 연구. 식품의약품안전청연보 1: 242-249