Transactions on Electrical and Electronic Materials

The Korean Institute of Electrical and Electronic Material Engineers (한국전기전자재료학회)
권호 표지
DOI QR코드

DOI QR Code

Synthesization of ZnO nanomaterials

  • Lee, Jong-Soo (Department of Electrical Engineering, College of Engineering, Korea University) ;
  • Min, Byung-Don (Department of Electrical Engineering, College of Engineering, Korea University) ;
  • Kim, Sang-Sig (Department of Electrical Engineering, College of Engineering, Korea University)
  • Published : 2003.10.01
Download PDF
⟨ Previous Next ⟩

Abstract

ZnO nanobelts, nanorods, and nanowires were synthesized at three different substrate temperatures from the thermal evaporation of ball-milled ZnO powders at 1380$^{\circ}C$. Transmission electron microscopy (TEM) revealed that the ZnO nanobelts are single crystalline with the growth direction perpendicular to the (010) lattice planes, and that the ZnO nanorods and nanowires are single crystalline with the growth directions perpendicular to the (001) and (110) lattice planes, respectively. In cathodoluminescence (CL), the peak energy of near bandedge (NBE) emission was determined for nanobelts, nanorods, and nanowires.

Keywords

References

  1. J. M. Hvam, 'Temperature induced wavelength shift of electron beam pumped laser from CdSe, CdS, and ZnO', Phys. Rev., Vol. B4, No. 12, p. 4459, 1971
  2. R. F. Service, 'Will UV lasers beat the blues?',Science, Vol. 276, No. 5314, p. 895, 1997 https://doi.org/10.1126/science.276.5314.895
  3. M. H. Huang, S. Mao, H. Feick, H. Yan, Y. Wu, H.Kind, E. Weber, R. Russo, and P. Yang, 'Room-temperature ultraviolet nanowire nanolasers', Science, Vol. 292, No. 5523, p. 1897, 2001 https://doi.org/10.1126/science.1060367
  4. Y. F. Chen, D. M. Bagnall, H. Koh, K. Park, K. Hiraga, Z. Zhu, and T. Yao, 'Plasma assisted molecular beam epitaxy of ZnO on c-plane sapphire: growth and characterization', J. Appl. Phys., Vol. 84, No. 7, p. 3912, 1998 https://doi.org/10.1063/1.368595
  5. D. M. bagnall, Y. F. Chen, Z. Zhu, T. Yao, M. Y. Shen, and T. Goto, 'High temperature excitonic stimulated emission from ZnO epitaxial layers', Appl. Phys. Lett, Vol. 73, No. 8, p. 1038, 1998 https://doi.org/10.1063/1.122077
  6. N. Hamada, S. Sawada, and A. Oshiyama, "New one dimensional conductors:graphitic microtubles', Phys. Rev. Lett, Vol. 68, No. 10, p. 1579, 1992 https://doi.org/10.1103/PhysRevLett.68.1579
  7. W. Han, S. Fan, Q. Li, and Y. Hu, 'Synthesis of gallium nitride nanorods through a carbon nanotube confined reaction', Science, Vol. 277, No. 5330,p.1287,1997 https://doi.org/10.1126/science.277.5330.1287
  8. J. Y. Li, X. L. Chen, Z. Y. Qiao, Y. G. Cao, and Y. C. Lan, 'Formation of GaN nanorods by a sublimination method', J. Cryst. Growth, Vol. 213, No. 3-4, p. 408, 2000 https://doi.org/10.1016/S0022-0248(00)00390-0
  9. W. S. Shi, Y. F. Zheng, N. Wang, C. S. Lee, and S. T. Lee, 'Microstructures of gallium nitride nanowires synthesized by oxide assisted method', Chem. Phys. Lett., Vol. 345, No. 5-6, p. 377, 2001 https://doi.org/10.1016/S0009-2614(01)00882-X
  10. X. Duan, Y. Huang, Y. Cui, J. Wang, and C. M. Lieber, 'Indium phosphide nanowires as building blocks for nanoscale electronic and optoelectronic devices', Nature, Vol. 409, No. 6816, p. 66, 2001 https://doi.org/10.1038/35051047
  11. Z. W. Pan, Z. R. Dai, and Z. L. Wang, 'Nanobelts of semiconducting oxides', Science, Vol. 291, No. 5510, p. 1947, 2001 https://doi.org/10.1126/science.1058120
  12. M. H. Huang, Y. Wu, H. Feick, N. Tran, E. Weber, and P. Yang, 'Catalytic growth of zinc oxide nanowires by vapor transport', Adv. Mater., Vol. 13, No. 2, p. 113, 2001 https://doi.org/10.1002/1521-4095(200101)13:2<113::AID-ADMA113>3.0.CO;2-H
  13. H. Z. Zhang, Y. C. Kong, Y. Z. Wang, X. Du, Z. G. Bai, J. J. Wang, D. P. Yu, Y. Ding, Q. L. Hang, and S. Q. Feng, '$Ga_{2}O_{3}$ nanowires prepared by physical evaporation', Solid State Communication, Vol. 109, No.11, P. 677, 1999 https://doi.org/10.1016/S0038-1098(99)00015-0
  14. B. C. Kim, K. T. Sun, K. S. Park, K. J. Im, T. Noh, M. Y. Sung, S. Nahm, Y. N. Choi, S. S. Park, and S. Kim, '$\beta$-$Ga_{2}O_{3}$ nanowires synthesized from milled GaN powders', Appl. Phys. Lett., Vol. 80, No. 3, p. 479, 2002 https://doi.org/10.1063/1.1435073
  15. J.S. Lee, K. Park, S. Nahm, S. Kim, and S. Kim, '$Ca_{2}O_{3}$ nanomatehals synthesized from ball milled GaN powders', J. Crys. Growth, Vol. 244, No. 3-4, p. 287, 2002 https://doi.org/10.1016/S0022-0248(02)01656-1
  16. K. Park, J. -S. Lee, M. -Y. Sung, and S. Kim, 'Structural and optical properties of ZnO nanowires synthesized from ball-milled ZnO powders', Jpn. J. Appl. Phys., Vol. 41, p. 7317, 2002 https://doi.org/10.1143/JJAP.41.7317