Bulletin of the Korean Chemical Society

Korean Chemical Society (대한화학회)
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Two-Dimensional Nickel Coordination Polymers: Ni(OBC)(bipyen)]·H2O and [Ni(NDC)(bipyen)(H2O)] (NDC = 2,6-Naphthalenedicarboxylate; OBC = 4,4'-Oxybis(benzoate); bipyen = trans-1,2-Bis(4-pyridyl)ethylene)

  • Lee, Yeon-Kyoung (Department of Chemistry (BK21), Sungkyunkwan University) ;
  • Lee, Soon W. (Department of Chemistry (BK21), Sungkyunkwan University)
  • Published : 2003.07.20
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Abstract

Hydrothermal reactions of Ni(NO₃)₂· 6H₂O with trans-1,2-bis(4-pyridyl)ethylene (bipyen), in the presence of a linear 2,6-naphthalene dicarboxylic acid (NDCH₂) and a bent 4,4'-oxybis(benzoic acid) (OBCH₂), gave a 2-D coordination polymer [Ni(NDC)(bipyen)(H₂O)] (1) and also a 2-D coordination polymer [Ni(OBC)(bipyen)]· H₂O (2), respectively. A reversible de-coordination and re-coordination of an aqua ligand was observed for polymer 1. Polymer 2 has an undulated 2-D network based on 50-membered rectangular grids, each of which has the dimension of 13.61 × 13.17 Å.

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