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Synthesis of Ultra Eine MnxZn1-xFe2O4(x = 0.69~0.74) Powder and Its Magnetic Properties

초미립 MnxZn1-xFe2O4(x = 0.69~0.74)분말의 제조 및 자기적 성질

  • Kwak, Jae-Eun (Department of Metallurgy and Materials Engineering, Hanyang University) ;
  • Lee, Wan-Jae (Department of Metallurgy and Materials Engineering, Hanyang University)
  • 곽재은 (한양대학교 공학대학 금속재료공학과) ;
  • 이완재 (한양대학교 공학대학 금속재료공학과)
  • Published : 2002.12.01

Abstract

$MnxZn_{1-x}Fe_2O_4$ (x=0.69~0.74) powders synthesized by the thermal decomposition of organic acid salts. The obtained powders were uniform in composition and ultra-fine particle with about 400 nm. The amount of spinel phase of these powders was about 50% in X-ray diffraction patterns. The calcination of powder was carried out at $900^{\circ}C$ for 2 hours in air. After the powders were calcined. the mean size of powder was about 500 nm and the amount of spinel phase was increased over about 65%. The maximum amount of spinel phase was about 75% in the specimen of X=0.72. The magnetic properties of calcined $Mn_{0.72}Zn_{0.28}Fe_2O_4$ powders were the best among the different among the different compositions.

Keywords

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