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A Study of Synthesis of NiCuZn-Ferrite Sintering in Low Temperature by Metal Nitrates and its Electromagnetic Property

  • 발행 : 2002.06.01

초록

The initial NiCuZn synthetic ferrite were acquired from thermally decomposing the metal nitrates $Fe(NO_3)_39H_2O, Zn(NO_3)_26H_2O, Ni(NO_3)_26H_2O, and Cu(NO_3)_23H_2O$ at $150^circ{C}$ for 24 hours, and then we calcined the synthetic powder at $500^circ{C}$, pulverized each of those for 3, 6, 9, 12, and 15 hours in a steel ball mill, sintered each at $700^circ{C}$ to $1,000^circ{C}$ for 1 hour, and thus studied their microstructures and electromagnetic properties. We could make the initial specimens chemically bonded in liquidity at a low-temperature $150^circ{C}$, by using the low melting points less than $200^circ{C}$ of the metal nitrates instead of the mechanical ball-mill pulverization, then narrow a distance between the particles into a molecular one, and thus lower the reaction point of sintering by at least $200^circ{C}$ to $300^circ{C}$. Their initial permeability was 50 to 400 and their maximum magnetic induction density and coercive force, 2,400 G and 0.3 Oe to 0.5 Oe respectively, which was similar to those of NiZnCu ferrite synthesized in the conventional process. In the graph of initial permeability by frequencies, a $180^circ{C}$ rotation of the magnetic domains which appears in a broad band of micro-wave before and after the resonance frequency, could be perceived.

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참고문헌

  1. Soft Ferrites/properties and applications 2nd ed v.1 Soft Ferrites/properties and applications 2nd ed E. C. Snelling
  2. Ferrites: Proc. of ICF6 v.1202 Ferrites: Proc. of ICF6 H. Momoi;A. Nakano;T. Nomura
  3. J. Am. Ceram. Soc. v.77 no.11 J. Am. Ceram. Soc. Masayuki Fujimoto https://doi.org/10.1111/j.1151-2916.1994.tb04517.x
  4. Ferrites: Proc. of ICF8 v.1117 Ferrites: Proc. of ICF8 A. Nakano;T. Aoki;H. Momoi;T. Suzuki;T. Nomura
  5. Ferrites: Proc. of ICF8 Ferrites: Proc. of ICF8 N. Taguchi;t. Yamaguchi;Y. Okino;H. Kishi
  6. IEEE Trans Magn v.31 no.6 IEEE Trans Magn J. H. Nam;H. H. Jung;J. Y. Shin;J. H. Oh https://doi.org/10.1109/20.489838
  7. Ferrites: Proc. of ICF8 Ferrites: Proc. of ICF8 Lu Mingyue
  8. J. of Kor. Mag. Soc. v.11 no.5 J. of Kor. Mag. Soc. J. H. Lee;J. G. Koh
  9. Am. Ceram. Bull v.60 no.2 Am. Ceram. Bull D. W. Johnson.Jr
  10. IEEE Tran. Magnn. v.36 no.5 IEEE Tran. Magnn. Suzilene R. Janasi;Daiel Rodrigurs;Fernando J. G. Landgraf;Mafilia Emura https://doi.org/10.1109/20.908788
  11. J. of Kor. Inst. of Metals v.28 no.11 J. of Kor. Inst. of Metals R. E. Park;N. K. Kang;K. H. Park;J. H. Oh
  12. IEEE Trans. Magn v.37 no.4 IEEE Trans. Magn W. C. Kim;S. J. Kim;Y. R. Uhm;C. S. Kim https://doi.org/10.1109/20.951173
  13. J. of Kor. Cer. Soc v.37 no.5 J. of Kor. Cer. Soc Y. J. Oh;H. S. Choi;J. Y. Choi
  14. J. of Kor. Mag. Soc v.11 no.4 J. of Kor. Mag. Soc S. Y. Ann;G. J. Yang;Y. G. Ryu
  15. J. of Magnetics v.5 no.4 J. of Magnetics W. C. Kim;Y. S. Yi;C. S. Kim
  16. J. of Kor. Cer. Soc. v.24 no.1 J. of Kor. Cer. Soc. K. H. Yi;B. H. Yi;S. G. Kim
  17. Kor. J. of Materials Research v.10 no.3 Kor. J. of Materials Research J. S. Kim;J. R. Ann;H. J. Ryu
  18. J. of Japan Inst. of Metals v.56 no.6 J. of Japan Inst. of Metals T. Asaka;Y. Okazawa;K. Tachikawa
  19. J. of Japan Inst. of Metals v.56 no.6 J. of Japan Inst. of Metals T. Asaka;Y. Shiomi;K. Tachikawa
  20. J. of Kor v.2 no.1 Powder Metallurgy Inst J. W. Jung;W. J. Yi
  21. Kor. J. of Materials Research v.5 no.5 Kor. J. of Materials Research J. W. Jung;W. J. Yi.
  22. J. of Kor v.2 no.1 Powder Metallurgy Inst. J. W. Jung;W. J. Yi
  23. Analysis of X-ray diffraction Analysis of X-ray diffraction Kato;M. J. Kim;I. H. Seo
  24. Elements of X-Ray Diffraction 2nd ed Elements of X-Ray Diffraction 2nd ed B. D. Cullity
  25. J. of Kor. Inst. of Electrical and Electronic Materials Engineeris v.8 no.6 J. of Kor. Inst. of Electrical and Electronic Materials Engineeris H. W. Cho;S. B. Jin;H. W. Moon;Y. J. Shin;
  26. Physics of Ferronmagnetism 2nd ed Physics of Ferronmagnetism 2nd ed Soshin Chikazumi
  27. Handbook of Modern Ferromagnetic Materials Handbook of Modern Ferromagnetic Materials Alex Goldman
  28. Basics and Applications of Magnitic Physics Basics and Applications of Magnitic Physics J. G. Koh;J. M. Song
  29. Basics and Applications of Magnitic Physics Basics and Applications of Magnitic Physics J. G. Koh;J .M. Song