Bulletin of the Korean Chemical Society

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Synthesis of a $^{13}$C-Labeled Oligomer: Solid-State NMR and Theoretical Studies

  • Published : 20011200
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Abstract

Keywords

References

  1. Macromolecules v.13 Hummel, J. P.;Flory, P. J.
  2. Mol. Cryst. Liq. Cryst. v.80 Birner, P.;Kugler, S.;Simon, K.;Naray-Szabo, G.
  3. J. Mater. Chem. v.6 Lee, M.;Oh, N. K.
  4. J. Am. Chem. Soc. v.120 Lee, M.;Cho, B. K.;Kim, H.;Yoon, J. Y.;Zin, W. C.
  5. Macromolecules v.34 Lee, M.;Cho, B. K.;Oh, N. K.;Zin, W. C.
  6. Macromolecules v.27 Han, C. D.;Chang, S.;Kim, S. S.
  7. Macromolecules v.28 Hardouin, F.;Sigaud, G.;Achard, M. F.;Brulet, A.;Cotton, J. P.;Yoon, D. Y.;Percec, V.;Kawasumi, M.
  8. Macromol. Symp. v.101 Wengner, G.
  9. Polymer v.35 Silvestri, R. L.;Koenig, J. L.
  10. Macromolecules v.28 Lesien, J.;Boeffel, C.;Spiess, H. W.;Yoon, D. Y.;Sherwood, M. H.;Kawasumi, M.;Percec, V.
  11. Macromolecules v.30 Ishida, H.;Kaji, H.;Horii, F.
  12. Macromolecules v.33 Yu, S. C.;Choi, Y.;Yu, K. H.;Yu, J.;Choi, H.;Kim, D. H.;Lee, M.
  13. ¹H NMR (CDCl₃) of 10: δ 1.42 (t, 3H, CH₂CH₃, J = 7.2 Hz), 3.37 (s, 3H, CH₃O), 3.50-3.75 (m, 44H, OCH₂), 3.90 (t, 2H, OCH₂CH₂OPh, J = 5.1 Hz), 4.20 (t, 2H, OCH₂-CH₂OPh, J = 5.1 Hz), 4.41 (q, 2H. OCH₂CH₃), 7.04 (d, 2H, Ar-H, J = 8.7 Hz), 7.35 (d, 2H, Ar-H, J = 8.8 Hz), 7.60-7.70 (m, 4H, Ar-H,), 7.63-7.80 (m, 6H, Ar-H), 8.12 (d, 2H, Ar-H, J = 8.5 Hz), 8.25 (d, 2H, Ar, J = 8.4 Hz).
  14. Bull. Korean Chem. Soc. v.21 Kim, D. H.;Eun, H. M.;Choi, H. S.
  15. J. Chem. Phys. v.85 Chesnut, D. B.;Forey, C. K.

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