Journal of the Korean Magnetic Resonance Society (한국자기공명학회논문지)

Korean Magnetic Resonance Society (한국자기공명학회)
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Complete assignments of $^{1}H$ and $^{13}C NMR$ spectra of Chivosazole F

  • Park, Jung-Rae (Marine Natural Products Chemistry Laboratory, Korea Ocean Research & Development Institute) ;
  • Jongheonn Shin (Marine Natural Products Chemistry Laboratory, Korea Ocean Research & Development Institute) ;
  • Kim, Jin-Cheol (Korea Research Institute of Chemical Technology) ;
  • Ahn, Jong-Woong (Korea Research Institute of Chemical Technology)
  • Published : 2001.12.01
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Abstract

The $^1$H and $^{13}$ C NMR spectra of chivosazole F from Sorangium cellulosum were completely assigned by a combination of ID and 2D NMR techniques. The configurations of double bonds were confirmed from the ROESY spectra. The stereochemistry at asymmetric carboncenters was partially assigned on the basis of the results of NOE analysis.

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