Metallurgical Study of Microconstituents in Transient Liquid Phase Bended Joints of Ni Base Superalloy

Ni기 초내열합금의 액상확산접합부 생성상의 금속조직학적 검토

  • 김대업 (현대 MOBIS(주) 기술연구소)
  • Published : 2001.02.01

Abstract

The metallurgical study of microconstituents in transient liquid phase bonded joints of Ni-base single crystal superalloys, CMSX-2 and CMSX-4 was investigated employing MBF-80 insert metal. TLP bonding of specimens was carried out at 1,373~1,523K for 0~19.6ks in vacuum. Three types of microconstituents ; needle-like constituent, dot-like constituent and abnormal shape constituent were formed in the bonded interlayer during TLP bonding operation. All these microconstituents were identified as boride. Microconstituents contain a large percentage of Cr in the early stage of bonding. As increasing the holding time, the amount of Cr was decreased and the amount of W, Co and Re were increased. From the analysis results of electron diffraction pattern by TEM, composition of elements in microconstituents were into MBlongrightarrowM$_{5}$B$_3$longrightarrowM$_2$B type with the increased in holding time. It can be explained by the fact that the relative amount of boron in microconstituents was decreased when the holding time was increased.d.

Keywords

References

  1. Proceedings of International Conference on High Temperature Alloys for Power Engineering D.J. Frasier;J.R.Whetstone;K. Harris;G.L. Ericson;R.E. Schwer
  2. Proceedings of International Conference on High Temperature Alloys for Power Engineering H. Harada;T.Yamagata;S. Nakazawa;K. Ohno;M. Yamazaki
  3. 耐熱金屬材料第123委員會硏究報告 v.34 no.3 合金設計プロぐラムによる單結晶超合金の組織と特性の解析 原田;橫川;大野;山縣;山崎
  4. Welding Journal v.53 no.4 TLP Bonding: A New Method for Joining Heat Resistant Alloys D.S.Duvall;W.A. Owczarski;D.F. Paulonis
  5. 溶接學會誌 v.49 no.7 各種Ni基礎合金のTLP接合性の比較 鈴村;恩澤;田村
  6. 鐵と鋼 v.72 no.13 Ni基礎合金單結晶の液相擴散接合界面 平根;吉成;森本
  7. 日本金屬學會誌 v.59 no.3 Ni基單結晶耐熱合金 TMS26の擴散接合部に及ぼすれじり角の影響 大橋;目黑;山縣
  8. 대한용접학회 춘계학술발표개요집 v.33 단결정 액상확산접합부의 생성상 거동 김대업;강정윤
  9. 대한 용접학회지 v.18 no.5 액산확산접합용 인서 트금속의 화학조성 최적화에 관한 연구 김대업;정승부;강정윤
  10. 대한용접학회지 v.9 no.4 304 스테인리스강과 구조용 탄소강의 천이액상확산접합에 관한 연구 강정윤;박노식;김우열;박세윤
  11. 溶接學會論文集 v.7 no.2 液相インサ一ト金屬擴散接合における等溫凝固過程の解析 中尾;西本;篠崎;姜
  12. Welding in the World v.41 no.2 Bonding phenomena and joint properties of transient liquid phase bonding of Ni-base single crystal superalloys D.Kim;K. Nishimoto;K. Saida;S. Asai;Y. Furukawa;Y. Nakao