한국식품영양과학회지 (Journal of the Korean Society of Food Science and Nutrition)
- 제29권4호
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- Pages.568-574
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- 2000
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- 1226-3311(pISSN)
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- 2288-5978(eISSN)
자동산화에 의한 Phytofluene으로부터 산화개열산물의 생성
Formation of Oxidative Cleavage from Phytofluene by Autoxidation
초록
Phytofluene를 dichloromethane에 용해하고 dry ice 상에서 ozonolysis를 행하였다. Ozonolysis에 의해 생성된 화합물은 silica gel chromatography를 행 하여 분획하고, photodiode array detector를 이용하여 ODS-HPLC로 분석하였다. Phytofluene을 5% Tween 40 수용액에 용해하고 37
Phytofluene was subjected to ozonolysis in ice-cold dichloromethane. The ozonolysis products were fractionated with a silica column and the carbonyl fraction was analyzed by ODS-HPLC with a photodiode array detector. Phytofluene was solubilized in 5% tween 40, and then oxidized by incubating under dim yellow light at 37