Polymer carrier 효과에 의하여 단순화된 새로운 세라믹분말 제조방법

A preparation of dysprosium monotitanate powder by mixed-oxide ceramics processing employing polymer carrier

  • 이상진 (일리노이 주립대학 재료공학과)
  • 발행 : 1998.04.01

초록

Ethylene glycol을 polymeric carrier로 사용한 새로운 화학적 세라믹 분말 제조 공정에 의하여 $(Dy_2TiO_5)$ 분말을 제조하였다. Chelation 공정의 생략에도 불구하고, 고순도의 미세한 입자를 갖는 세라믹 분말 제조가 가능함을 확인하였다. 열분석, 미세구조분석, 회절분석 등으로 분말특성을 평가하였다.

Dysprosium monotitanate $(Dy_2TiO_5)$ powder was synthesized by a simple mixed-oxide ceramics process using ethylene glycol (EG). Ethylene glycol, as the organic carrier for the metal cations, was used for polymerization mechanism. The successful used of a non-chelating polymer for the mixed-oxide ceramic process indicated that cation chelation is not the only route for creating stable ceramic precursors. Characterization of the powders by various thermal analysis, microscopy, and diffraction methods has been carried out.

키워드

참고문헌

  1. U.S. Pat. No. 3, 330, 697 M. Pechini
  2. Mater. Res. Soc. Symp. Proc. v.32 D. Budd;D.A. Payne
  3. Ceramic Transactions v.62 M.A. Gulgun;W.M. Kriven;J.J. Kingsley(ed.);C.H. Schilling(ed.);J.H. Adair(ed.)
  4. Handbook of Water-Soluble Gums and Resins R.L. Davidson;R.L. Davidson(ed.)
  5. Polyvinyl Alcohol Properties and Applications K. Toyoshima;C.A. Finch(ed.)
  6. J. Am. Ceram. Soc. S.J. Lee;W.M. Kriven
  7. Chemical Synthesis of Advanced Ceramic Materials D. Segal;S. Segal(ed.)
  8. Acta Crystallogr. v.B24 W.G. Mumme;A.D. Wadsley
  9. Izv. Akad. Nauk SSSR, Neorg. Mater. v.18 M.A. Petrova;D.P. Romanov;R.G. Grebenshchikov