Molecular Structure abd Stereochemical Assignment of 3-phenyl-5-(2-naphthyl)-1,2,4-trioxolane-3-carbonitrile

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14. Data for cystallographic studies were measured on a MAC sciences MXC3 fourcircle diffractometer. The unit cell and other related parameters of compounds (5) are as follows; F. W.=303.32;; Colorless polyhedral; Crystal demension=1.80×0.80×0.40× mm³; Space group $C_{2h}^5$-P2₁/n;a=18.214(5) Å, b=7.416(2) Å, c=1.037(3)Å,β=108.49(2) Å,V=1542.1(2) ų;Z=4;$D_{calc}$=1.337 g/㎤;Radiation=Mokα, λ=0.71073 Å; Temperature=293(2)K; final R=0.0539; Number of unique reflections=1982