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Molecular Structure abd Stereochemical Assignment of 3-phenyl-5-(2-naphthyl)-1,2,4-trioxolane-3-carbonitrile

  • 발행 : 1996.04.20

초록

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참고문헌

  1. Ozonation in Organic Chemistry v.1 Baily, P. S.
  2. Justus Liebigs Ann. Chem. v.561 Criegee, R.;Wenner, G.
  3. J. Am. Chem. Soc. v.96 Lattimer, P. R.;Kuczkowski, R. L.;Gillies, C. W.
  4. J. Am. Chem. Soc. v.100 Bailey, P. S.;Ferrel, T. M.
  5. J. Mol. Spectroscopy v.65 Mazur, W.;Kuczkowski, R. L.
  6. J. Am. Chem. Soc. v.64 Kuczkowski, R. L.;Gilles, C. W.;Gallaher, K. L.
  7. J. Am. Chem. Soc. v.89 Murray, R. W.;Youssefyeh, R. D.;Story, P. R.
  8. J. Am. Chem. Soc. v.87 Loan, L. D.;Murray, R. W.
  9. Chem. Ber. v.104 Criegeem R.;Korber, H.
  10. Magnetic Reson. Chem. v.24 Choe, J.-I;Choi, H.-S.;Kuczkowski, R. L.
  11. Liebigs Ann. Griesbaum, K.;Ovez, B.;Huh, T. S.;Dong, Y.
  12. Liebigs Ann Griesbaum, K.;Ball, V.;Beck, J.;McCullough, K.
  13. J. Org. Chem. v.56 Griesbaum, K.;Krieger-Beck, P.;Beck, J.
  14. Data for cystallographic studies were measured on a MAC sciences MXC3 fourcircle diffractometer. The unit cell and other related parameters of compounds (5) are as follows; F. W.=303.32;; Colorless polyhedral; Crystal demension=1.80×0.80×0.40× mm³; Space group $C_{2h}^5$-P2₁/n;a=18.214(5) Å, b=7.416(2) Å, c=1.037(3)Å,β=108.49(2) Å,V=1542.1(2) ų;Z=4;$D_{calc}$=1.337 g/㎤;Radiation=Mokα, λ=0.71073 Å; Temperature=293(2)K; final R=0.0539; Number of unique reflections=1982