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Oxidation Stability of PAO Oils Determined by Differential Scanning Calorimetry

  • Shim, Joosup (Korea Research Institute of Chemical Technology) ;
  • Cho, Wonoh (Korea Research Institute of Chemical Technology) ;
  • Chung, Keunwo (Korea Research Institute of Chemical Technology)
  • Published : 1996.03.01

Abstract

The suitability of a pressure differential scanning calorimetry (PDSC) in monitoring the quality of synthetic base fluids has been investigated using polyalphaolefin (PAO) oils as an example. Induction period meassured at 170, 180 and 19$0^{\circ}C$, and 3.53 MPa oxygen pressure was applied to characterize their oxidation stability. The PDSC method has proven to be simple and repeatable and requires only small sample size for testing. More importantly, it can be applied in differentiating the oxidation performance quality of PAO oils and is versatile enough for use in studying kinetic aspects of PAO oil oxidation which include the effect of temperature and antioxidant concentration. Additionally, the method appears to correlate well with a rotary bomb oxidation test (RBOT).

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References

  1. J. Inst. of Petroleum v.57 The Characteristics of Lube Oils and Fuel Oils by DSC Analysis Noel, F.
  2. SAE Tech. Paper 801383 Characterization of Lubricating Oils by Differential Scanning Calorimetry Walker, J.A.;Tsang, W.
  3. SAE Tech. Paper 821252 Evaluation of Automotive Crankcase Lubricants by Differential Scanning Calorimetry Hsu, S.M.;Cummings, A.L.;Clark, D.B.
  4. J. of Synthetic Lubrication v.5 DSC-Cell: A Versatile Tool to Study Thermo-Oxidation of Aviation Lubricants Zeman, A.