Synthesis of N-p-Nitrophenyl Poly(m-Phenylene Isophthalamide

N-p-Nitrophenyl Poly(m-Phenylene Isophthalamide)의 합성

  • Hongbum Kim (Department of Chemistry, College of Science, Dongguk University) ;
  • Donghyun Kim (Department of Chemistry, College of Science, Dongguk University) ;
  • Jaewung Lee (Department of Chemistry, College of Science, Dongguk University) ;
  • Sangyeop Song (Department of Chemistry, College of Science, Dongguk University) ;
  • Nakjoong Kim (Polymer Chemistry Laboratory, Korea Institute of Science and Technology)
  • 김홍범 (동국대학교 이과대학 화학과) ;
  • 김동현 (동국대학교 이과대학 화학과) ;
  • 이재웅 (동국대학교 이과대학 화학과) ;
  • 송상엽 (동국대학교 이과대학 화학과) ;
  • 김낙중 (한국과학기술원 고분자설계연구실)
  • Published : 1993.02.20

Abstract

N-p-nitrophenyl poly(m-phenylene isophthalamide) was obtained from treatment of poly(m-phenylene isophthalamide) with sodium hydride in dimethyl sulfoxide followed by the addition of 1-fluoro-4-nitrobenzene in 43 wt% yield. Its inherent viscosity was 0.606 g/cm${\cdot}$sec determined from a solution of 0.125 g of the above polymer dissolved in 25 ml of 98% sulfuric acid at $30^{\circ}C.$ In order to synthesize poly(m-phenylene isophthalamide), 1,3-phenylenediamine is allowed to react with isophthaloyl chloride in chloroform in the presence of triethylamine and added triethylamine hydrochloride. The value of inherent viscosity is 0.560 g/cm${\cdot}$sec measured at the same condition. The substitution ratio of N-p-nitrophenyl poly(m-phenylene isophthalamide) was to be 16.7∼47.0% by using the $^1H-NMR$ integration. When the higher inherent viscosity of poly(m-phenylene isophthalamide) was used, lower substitution ratio would be calculated.

N-p-nitrophenyl poly(m-phenylene isophthalamide)는 poly(m-phenylene isophthalamide)를 디메틸술폭사이드(DMSO) 용매속에서 수소화나트륨(NaH)과 반응시킨 후, 1-fluoro-4-nitrobenzene을 첨가하여 43 wt%를 얻었다. 고유점성도는 폴리머를 98% 황산에 녹여 $30^{\circ}C$에서 측정하였으며 그 값은 0.606g/cm${\cdot}$sec(0.125g/25ml)였다. Poly(m-phenylene isophthalamide) 합성에 있어서, 1,3-페닐디아민은 트리에틸아민과 트리에틸아민·염화수소가 있는 클로로포름 용매속에서 클로로이소프탈산과 반응에 의해 얻어졌다. 고유 점성도 값은 같은 조건에서 0.560g/cm${\cdot}$sec 였다. N-p-nitrophenyl poly(m-phenylene isophthalamide)의 치환비율은 $^1H-NMR$ integration에 의해 16.7~47.0%였다. 고유점성도가 큰 poly(m-phenylene isophthalamide)를 사용했을 때는 치환비율이 낮았다.

Keywords

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