Effect of Surface Grinding on Low Temperature Degradation of 3Y-TZP

표면 연마가 3Y-TZP의 저온열화에 미치는 영향

  • 김대준 (한국과학기술연구원 재료연구단) ;
  • 이홍림 (연세대학교 세라믹공학과) ;
  • 정형진 (한국과학기술연구원 재료연구단)
  • Published : 1993.02.01

Abstract

Grinding of 3mol% Y-TZP enhanced the texturing of t-ZrO2, which is represented by the increased I(002)t/I(200)t peak intensity ratio, and an asymetric broadening of (111)t peak. The degree of texturing and asymetric broadening depended on a seversity of grinding. The asymetric (111)t peak broadening was resulted by the formation of r-ZrO2. When aged at 25$0^{\circ}C$ for 120h, r-ZrO2 transformed to t-ZrO2 due to the relief of stressed surface area and the amount of tlongrightarrowm transformation inversely varied with the I(002)t/I(200)t. The inverse dependence was interpreted by that the degree of texturing determines the magnitude of residual surface stress and the lattice relaxation of t-ZrO2, which causes the low temperature degradation, is retarded as the residual stress becomes greater.

Keywords

References

  1. J. Am. Cerm. Soc. v.69 no.10 Ferroelastic Domain Switching as a Toughening Mechanism in Tetragonal Zirconia A.V. Virkar;R.L.K. Matsumoto
  2. Advances in Ceramics v.24B Toughening Mechanism in Tetragonal Zirconia Polycrystalline(TZP) Ceramics;Science and Technology of Zirconia Ⅲ A.V. Virkar;R.L.K. Matsumoto;S. Somiya(ed.);N. Yamamoto(ed.);H. Yanagida(ed.)
  3. J. Am. Ceram. Soc. v.72 no.11 Ferroelastic Domain Switching in Polydomain Tetragonal Zirconia Single Crystals G.V. Srinviasan;J.-F. Jue;S.-Y. Kuo;A.V. Virkar
  4. J. Am. Ceram. Soc. v.73 no.12 Fabrication, Microstructural Characterization, and Mechanical Properties of Polyerystalline t'-Zirconia J.F. Jue;A.V. Virker
  5. J. Am. Ceram. Soc. v.73 no.6 Grinding-Induced Texture in Ferroelastic Tetragonal Zirconia K. Mehta;J.F.Jue;A.V. Virkar
  6. J. Am. Ceram. Soc. v.72 no.8 Metastability of the Martensitic Transformation in a 12mol% Ceria-Zirconia Alloy:Ⅱ, Grinding Studies M.V. Swain;R.H. Hannink
  7. Mat. Res. Soc. Symp. Proc. v.78 Texture on Ground, Fractured, and Aged Y-TZP Surfaces;Advanced Structural Ceramics F. Reidinger;P.J. Whalen;P.F. Becher(ed.);M.V. Swain(ed.);S. Somiya(ed.)
  8. J. Am. Ceram. Soc. v.71 no.8 Structural Changes by Mechanical and Thermal Stresses of 2.5mol%-Y₂O₃-Stabilized Tetragonal ZrO₂Polycrystals Y. Kitano;Y. Mori;A. Ishitani
  9. Mat. Res. Soc. Symp. Proc. v.78 A Study of Rhombohedral Phase in Y₂O₃-Partially Stabilized Zirconia;Advanced Structural Ceramics Y. Kitano;Y. Mori;A. Ishitani;T. Masaki;P.F. Becher(ed.);M.V. Swain(ed.);S. Somiya(ed.)
  10. J. Mater. Sci. Lett. v.2 Rhombohedral Phase Produced in Abraded Surfaces of Partially Stabilized Zirconia(PSZ) H. Hasegawa
  11. J. Mater. Sci. Lett. v.4 Cubic-to-Rhombohedral Phase Transformation in Zirconia by Ion Implantation H. Hasegawa;T. Hioki;O. Kamigaito
  12. J. Mater. Sci. Lett. v.2 The Rhombohedral Phase Produced in Partially-Stabilized Zirconia T. Sakuma;Y.-I. Yoshizawa;H. Suto
  13. Advances in Ceramics v.24A Characteristic Microstructure of CeO₂- and Y₂O₃-Doped Tetragonal Zirconia Polycrystals;Science and Technology of Zirconia Ⅲ K. Urabe;A. Nakajima;H. Ikawa;S. Udakawa;S. Somiya(ed.);N. Yamamoto(ed.);H. Yanagida(ed.)
  14. J. Am. Ceram. Soc. v.72 no.2 Prevention of Low-Temperature Surface Transformation by Surface Recrystallization in Yttria-Doped Tetragonal Zirconia P.J. Whalen;F. Reidinger;P.F. Antrim
  15. J. Am. Ceram. Soc. v.74 no.8 Low-Temperature Aging of t'-Zirconia: The Role of Microstructure on Phase Stability J.F. Jue;J. Chem; A.V. Virkar
  16. J. Am. Ceram. Soc. v.55 no.6 Phase Analysis in Zirconia Systems R.C. Garvie;P.S. Nicholson
  17. unpublished work D.-J. Kim
  18. Zirconia Ceramics v.4 Thermal Stability of Toughened Y-PSZ T. Kawanami;H. Ohnishi;S. Somiya(ed.);M. Yoshimura(ed.);Uchida Rokakuho(ed.)
  19. J. Am. Ceram. Soc. v.72 no.5 Structural Changes by Compressive Stresses of 2.0-mol%-Yttria-Stabilized Tetragonal Zirconia Polycrystals Y. Kitano;Y. Mori;A. Ishitani
  20. J. Am. Ceram. Soc. v.74 no.10 Texture from Domain Switching of Tetragonal Zirconias K.J. Bowman
  21. J. Am. Ceram. Soc. v.71 no.7 Domain Switching as a Toughening Mechanism in Tetragonal Zirconia B.-S. Li;J.-S. Cherng;KJ. Bowman;I.-W. Chen
  22. 한국요업학회지 v.29 no.8 $Ta_2O_5$ 첨가가 3mol% Y-TZP의 저온 열화에 미치는 영향 김대준;최두진