QUANTITATIVE ANALYSIS OF RESIDUAL MONOMERS IN VISIBLE LIGHT-CURED RESINS

치과용 가시광선중합형 복합레진의 잔류단량체 정량분석에 관한 연구

  • Choi, Kyoung-Kyu (Department of Conservative Dentistry, College of Dentistry, Kyung Hee University) ;
  • Min, Byung-Soon (Department of Conservative Dentistry, College of Dentistry, Kyung Hee University)
  • 최경규 (경희대학교 치과대학 보존학교실) ;
  • 민병순 (경희대학교 치과대학 보존학교실)
  • Published : 1992.03.31

Abstract

The purpose of this study was to estimate the contents of the residual monomers, such as Bis-GMA and TEGDMA. In this study, materials used were six kinds of anterior and posterior visible light-cured resins. Resins were placed in disk-shaped Teflon mold (8.5mm in diameter, 2.0mm in thickness), and cured for 20 seconds with visible light source attached wide diameter lightguide. The specimens were immersed in 10ml ethanol and stored for 5 days at $37^{\circ}C$. The concentration of residual monomers in eluate solution was analysed by HPLC, and the following results are obtained. 1. The residual Bis-GMA and TEGDMA were detected in all materials used, and the ranges of quantity of the residual Bis-GMA was 0.101-1.236 wt% and that of TEGDMA was 0.230-5.794 wt%.2. The contents of residual TEGDMA was detected higher than that of residual Bis-GMA (P < 0.01). 3. The content of residual monomers was detected to be highest in Bis-Fil M as microfilled type. 4. In most of the materials used, there was no significant difference in the contents of residual monomers between anterior and posterior light-cured resins.

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