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Intramolecular Proton Transfers of 2-hydroxy-4,5-naphthotropone

  • Du-Jeon Jang (Spectroscopy and Color Laboratroy, Korea Standards Research Institute)
  • Published : 1991.08.20

Abstract

The intramolecular proton transfers of 2-hydroxy-4,5-naphthotropone in room temperature solutions are studied using static and time-resolved absorption and emission spectroscopy. Dual normal and tautomer fluorescence is observed in ethanol solution, while only the tautomer fluorescence is observed in cyclohexane solution. The fluorescence lifetimes and quantum yields in ethanol and cyclohexane solutions indicate that in hydrocarbon solvents, rapid intersystem crossing competes with proton transfer in the first excited singlet state. Transient absorption spectra and kinetics indicate that proton transfer also undergoes in the first triplet state with a transfer time of ∼ 3 ns. No transient absorption from the tautomer ground state indicates a rapid back proton transfer in the ground state.

Keywords

References

  1. Adv. Photochem. v.10 W. Klopper
  2. J. Chem. Soc. Faraday Trans. v.82 M. Kasha
  3. Chem. Phys. Lett. v.148 F. Laermer;T. Elsaesser;W. Kaiser
  4. J. Chem. Phys. v.90 G. A. Brucker;D. F. Kelley
  5. J. Phys. Chem. v.93 P. F. Barbara;P. K. Walsh;L. F. Brus
  6. J. Am. Chem. Soc. v.112 J. Catalan;F. Fabero;M. S. Guijarro;R. M. Claramunt;M. D. S. Maria;M. C. Foces-Foces;F. H. Cano;J. Elguero;R. Sastre
  7. J. Phys. Chem. v.94 M. Itoh;Y. Fujiwara;M. Matsudo;A. Higashikata;K. Tokumura
  8. Photochem. Photobiol. v.28 R. Croteau;R. M. Leblanc
  9. J. Phys. Chem. v.89 D.-J. Jang;D. F. Kelley
  10. Ph. D. Dissertation, University of California S. C. Busman
  11. Ph. D. Dissertation, University of California D. Ngo
  12. J. Chem. Phys. v.80 D. F. Kelley;N. A. Abul-Haj;D.-J. Jang
  13. Rev. Sci. Instrum. v.56 D.-J. Jang;D. F. Kelly
  14. J. Phys. Chem. v.90 D.-J. Jang;G. A. Brucker;D. F. Kelley
  15. Phys. Chem. v.88 D. McMorrow;M. J. Kasha
  16. Analyst v.85 C. A. Parker;W. T. Rees
  17. J. Chem. Soc., Faraday Trans. 1 v.69 J. F. Ireland;P. A. H. Wyatt
  18. Disc. Far. Soc. v.39 T. S. Godfrey;G. Porter;P. Suppan

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