DOI QR코드

DOI QR Code

A Study on Spin-Lattice Relaxation of Methyl Protons in 2,6-Dichlorotoluene and N-Methyl Phthalimide

  • Lee, Jo-Woong (Department of Chemistry, Seoul National University) ;
  • Lim, Man-Ho (Department of Chemistry, Seoul National University) ;
  • Rho, Jung-Rae (Department of Chemistry, Seoul National University)
  • Published : 1991.02.20

Abstract

Spin-lattice relaxation of methyl protons in 2,6-dichlorotoluene and N-methyl phthalimide, each dissolved in CDCl$_3$, has been studied at 34$^{\circ}$C and the contribution from spin-rotation interaction to the relaxation process has been separated from that due to dipole-dipole interactions among methyl protons. The results show that the spin-rotational contributions to the initial rate of relaxation in 2,6-dichlorotoluene and N-methyl phthalimide amount to 18 and 31%, respectively, of the total relaxation rate at 34$^{\circ}$C. The method of separating the spin-rotational contribution from that of dipolar interactions adopted in this paper is based on the well known fact that in an A$_3$ spin system such as methyl protons in liquid phase dipolar relaxation mechanism gives non-exponential decay of the z-component of total magnetization of protons while the random field fluctuation such as spin-rotational mechanism causes exponential decay.

Keywords

References

  1. Principles of Nuclear Magnetism A. Abragam
  2. Fourier Transform NMR Spectroscopy D. Shaw
  3. J. Chem. Phys. v.35 C. S. Johnson, Jr.;J. S. Waugh
  4. J. Chem. Phys. v.48 W. T. Huntress, Jr.
  5. The Theory of Nuclear Magnetic Relaxation in Liquids J. McConnell
  6. J. Magn. Res. v.6 R. G. Parker;J. Jonas
  7. J. Chem. Phys. v.52 K. F. Kuhlmann;D. M. Grant;R. K. Harris
  8. Nuclear Magnetic Resonance Spectroscopy R. K. Harris
  9. J. Magn. Res. v.2 T. E. Burke;S. I. Chan
  10. J. Magn. Res. v.33 W. Suchanski;P. C. Canepa
  11. Phys. Rev. v.131 P. S. Hubbard
  12. Chem. Phys. Lett. v.93 D. S. Chung;B. S. Kim;J. W. Lee;K. J. Shin
  13. J. Am. Chem. Soc. v.98 J. D. Cutnell;J. A. Glasel
  14. J. Magn. Res. v.19 J. F. Rodrigues de Miranda;C. W. Hilbers
  15. J. Chem. Phys. v.51 P. S. Hubbard
  16. J. Chem. Phys. v.52 P. S. Hubbard
  17. Adv. Magn. Res v.9 L. G. Werbelow;D. M. Grant;J. S. Waugh(ed.)
  18. Principles of Nuclear Magnetic Resonance in One and Two Dimensions R. R. Ernst;G. Bodenhausen;A. Wokaun
  19. J. Magn. Res. v.31 E. Haslinger;R. M. Lynden-Bell