DOI QR코드

DOI QR Code

The C$_4$ Photocycloadduct Formation of Khellin with Some Olefins

  • Ho Kwon Kang (Department of Agricultural Chemistry, Suncheon National University) ;
  • Sang Chul Shim (Department of Chemistry, Korea Advanced Institute of Science and Technology)
  • Published : 1989.12.20

Abstract

The photocycloaddition reaction of khellin with several olefins has been investigated. The photocycloadducts are formed regioselectively on furanyl 4',5'-double bond of khellin probably due to the localization of excitation energy on the furanyl 4',5'-double bond in the reactive excited state. The photocycloaddition reaction proceeds through the excited triplet state and the same product was formed when khellin is irradiated with dimethylfumarate or dimethylmaleate indicating the formation of common intermediate. The quantum yields of photocycloadduct formation, fluorescence, and intersystem crossing are very sensitive to proton-donating ability of solvents.

Keywords

References

  1. J. Am. Chem. Soc. v.72 A. Schonberg;A. Sina
  2. Biochim. Biophys. Acta v.475 E. Cassuto;N. Gross;E. Bardwell;P. Howard-Flanders
  3. Dermatologica v.165 A. Abdel-Fattah;M. N. Aboul-Enein;G. M. Wassel;B. S. El-Menshowi
  4. Photochem. Photobiol. v.39 B. Ortel;A. Tanew;K. Wolff;H. Honigsmann
  5. Biochemistry v.21 D. Kanne;K. Straub;H. Rapoport;J. E. Hearst
  6. J. Am. Chem. Soc. v.104 D. Kanne;K. Straub;J. E. Hearst;H. Rapoport
  7. Biochim. Biophys. Acta v.217 G. Rodighiero;L. Musajo;F. Dall'Acqua;S. Marciani;G. Caporale;L. Ciavatta
  8. Trends in Photobiology S. T. Issacs;C. Chun;J. E. Hoyle;H. Rapoport;J. E. Hearst;C. Helene(ed.)(et al.)
  9. Photochem. Photobiol. v.38 F. Abeysekera;Z. Abramowski;G. H. N. Towers
  10. Purification of Laboratory Chemicals(2nd ed.) D. D. Perrin;W. L. F. Armarego;D. R. Perrin
  11. Photochemistry(2nd ed.) J. G. Calvert;J. N. Pitts, Jr.
  12. Photochem. Photobiol. v.27 S. C. Shim;K. Y. Choi;P.-S. Song
  13. Korean Biochem. J. v.14 S. C. Shim;B. M. Lee
  14. Photochem. Photobiol. v.30 S. C. Shim;K. H. Chae
  15. Photochem. Photobiol. v.38 S. C. Shim;Y. J. Kim
  16. Photochem. Photobiol. v.40 S. C. Shim;Y. J. Kim;H. K. Kang
  17. Bull. Korean Chem. Soc. v.8 S. C. Shim;H. K. Kang