DOI QR코드

DOI QR Code

Fourier-Transform Infrared Studies of Ionomeric Blend and Ionic Aggregation

  • Lee, Sang-Koog (Department of Chemistry, Korea Advanced Institute of Science and Technology) ;
  • Jeon, Seung-Ho (Department of Chemistry, Korea Advanced Institute of Science and Technology) ;
  • Ree, Tai-Kyue (Department of Chemistry, Korea Advanced Institute of Science and Technology) ;
  • Sohn, Jeong-In (Department of Chemistry, Hallym University)
  • Published : 1986.08.20

Abstract

The ionomeric blend and the ionic aggregation studies by using a Fourier-transform infrared spectroscopy(FT-IR) are presented. Two ionomers were prepared, one is barium polyacrylate and the other is barium polystyrenesulfonate. The blend of the two ionomers of the barium salts shows intermolecular ionic interaction between the carboxylated ionomer and the sulfonated ionomer. This interaction leads to considerable differences between the spectrum of the blend and the sum of the spectra of the pure ionomers. From our results, it is shown that ionic interactions must play an important role in the compatibility of the two ionomers. In the ionic aggregation study, the bands due to asymmetric stretching mode of carboxylate anion(COO-) in the carboxylated ionomer and the ionomer blend increase in intensity with increasing the divalent barium cations. These results indicate the formation of ion pairs. The doublet due to the asymmetric stretching modes of the carboxylate anion(COO-) is concerned with a sort of local structure found in the ion aggregation. By considering a possible structure for multiplets in the blend, the spectral splitting and the frequency shift are well explained.

Keywords

References

  1. Polymer Blend v.1;2 D.R. Paul;S. Newman
  2. Polymer-Polymer Miscibility O. Olabisi;L.M. Robeson;M.T. Shaw
  3. Ionic Polymers L. Holliday
  4. J. Appl. Chem. Biotech. v.21 A.D. Wilson;B.E. Kent
  5. J. Polym. Sci., Polym. Lett. Ed. v.15 M.M. Coleman;J. Zarian;D.F. Varnell;P.C. Painter
  6. J. Polym. Sci., Polym. Phys. Ed. v.17 M.M. Coleman;J. Zarian
  7. J. Polym. Sci., Polym. Phys. Ed. v.18 M.M. Coleman;D.F. Varnell
  8. J. Polym. Sci., Polym. Phys. Ed. v.22 M. Miya;R. Iwamoto
  9. J. Polym. Sci., Polym. Phys. Ed. v.22 D. Garcia
  10. J. Polym. Sci., Polym. Phys. Ed. v.17 M.M. Coleman;J. Zarian
  11. J. Polym. Sci., Polym. Phys. Ed. v.21 B.A. Brozoski;M.M. Coleman;P.C. Painter
  12. Macromolecules v.14 S.R. Fahrenholtz;T.K. Kwei
  13. Appl. Spectrosc. v.35 B.A. Brozoski;P.C. Paintner;M.M. Tovar Rodriguez
  14. Macromolecules v.17 B.A. Brozoski;P.C. Painter;M.M. Coleman
  15. J. Polym. Sci., Polym. Phys. Ed. v.20 P.C. Painter;B.A. Brozoski;M.M. Coleman
  16. Macromolecules v.9 E.D. Andreeva;V.N. Nikitin;Y.M. Boyartchuk
  17. Macromolecules v.17 B.A. Brozoski;M.M. Coleman;P.C. Painter
  18. I & EC Product Research and Development v.1 no.4 A.F. Turbak
  19. J. Phys. Chem. v.72 W.J. Macknight;L.W. Mckena;B.E. Reed;R.S. Stein
  20. Crystal Structure R.W.G. Wyckoff
  21. Structural Inorganic Chemistry A. Wells
  22. Macromolecules v.17 J.A. Lefelar;R.A. Weiss

Cited by

  1. Self-Healing Asphalt Prepared by using Ionic Epoxy Resin vol.50, pp.3, 1986, https://doi.org/10.7473/ec.2015.50.3.167