Synthsis of $\beta$-Sialon from Hadong Pink Kaolin

하동카올린으로부터 $\beta$-Sialon의 합성

  • 이홍림 (연세대학교 공과대학 요업공학과) ;
  • 이형직 (연세대학교 공과대학 요업공학과)
  • Published : 1984.01.01

Abstract

$eta$-Sialon synthesis was investigated via the simultaneous reduction and nitridation of Hadong Pink Kaolin using the graphite as a reducing agent at 135$0^{\circ}C$ under 80% $N_2-20%H_2$ atmosphere. When Hadong Pink Kaolin-graphite-silicon nitride seed(molar ratio ; $SiO_2:C:Si_3N_4$=1;3.5:0.05) mixture was heated at 135$0^{\circ}C$ for as long as 20h in 80%$N_2-20%H_2$ atmosphere a homogeneous $eta$-Sialon$(Si_{3.5}Al_{2.5}O_{2.5}N_{2.5})$ was mainly formed together with a small amount of $\alpha$-$Si_3N_4$.

Keywords

References

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