Mullitization of Al-Kaolin Mixture

Al-Kaolin 혼합물의 Mullite화 반응

  • 박정현 (연세대학교 공과대학 요업공학과) ;
  • 조정식 (연세대학교 공과대학 요업공학과) ;
  • 배원태 (연세대학교 공과대학 요업공학과)
  • Published : 1983.02.01

Abstract

This research is aimed to synthesize the mullite by adding Al powder of $Al_2O_3$ to kaolin. Specimens fired at 1400, 1450 and 150$0^{\circ}C$ were compared in their X-ray diffraction patterns quantitative analysis of mullite formed and fine microstructures with those containing reactive $Al_2O_3$ activated $Al_2O_3$ as alumina source The experiment of Al oxdiation was also performed by measuring the weight increase of specimens. Two different shapes of mullites acicular and chunky were observed by SEM and the yield of mullites were in-creased by the order of adding activated $Al_2O_3$ reactive $Al_2O_3$ and Al powder to kaolin.

Keywords

References

  1. J. Kor. Ceram. Soc. v.10 no.2 1. A Study on the Manufacture of the Chamotte and Refractory Brick by a Domestic Kaolin, 2. A Fundamental Study on Synthesis of Mullite Lee Chong-Keun;Han Sang-Mok;Cho Hang-Keun;Kim Cheol-Young
  2. J. Kor. Ceram. Soc. v.13 no.4 Formation of Mullite and Effect of T₁O on Mullitization Jang Sung-Do;Jung Hyung-Jin;Moh Kyung-Hwa
  3. Trans. Brit. Ceram. Soc. v.78 no.6 Role of Magnesium Compounds on Mullitization of Clay-Alumina Mixtures Pranab Das
  4. セラミツクスの基礎 橋本謙 一;浜野健也
  5. J. Am. Ceram. Soc. v.52 no.2 Kinetics and Mechanism of High-Temperature Reactions of Kaolinite Minerals J. F. Duncan;K. J. D. Mackenzie
  6. J. Am. Ceram. Soc. v.42 no.7 The Kaolinite-Mullite Reaction Series:1. A Survey of Outstanding Problems, 2. Metakaolin, 3. The High Temperature Phases G. W. Brindley;M. Nakahira
  7. J. Elec. Chem. Soc. v.103 no.9 Natural and Thermally Formed Oxide Films on Aluminium M. S. Hunter;P. Fowle
  8. J. Elec. Chem. Soc. v.108 no.12 Oxidation of Molten High Purity Aluminium in Dry Oxygen W. C. Sleepy
  9. J. Am. Ceram. Soc. v.57 no.5 Existence of Mullite without Silica P. H. Duvigneaud
  10. The Principles of Engineering Materials C. R. Barrett;W. D. Nix;A. S. Tetelman
  11. J. Am. Ceram. Soc. v.59 no.7-8 Mullite Development from Fibrous Kaolin Mineral T. W. Campos;H. D. S. Santos;P. D. S. Santos
  12. J. Am. Ceram. Soc. v.61 no.1-2 Spectroscopic Investigations of the Kaolinite-Mullite Reaction Sequence M. Bulens;A. Leonard;B. Delmon
  13. Private Correspondence Kim. Hai-Doo
  14. High Temperature Oxides Refractory Glasses, Glass-Ceramics and Ceramics A. M. Alper
  15. J. Am. Ceram. Soc. v.53 no.5 Differential Thermal Calorimetric Determination of the Thermodynamic Properties of the Kaoiinite P. S. Nicholson;R. M. Fulrath