약학회지 (YAKHAK HOEJI)
- 제26권2호
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- Pages.129-132
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- 1982
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- 0377-9556(pISSN)
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- 2383-9457(eISSN)
GC/MS에 의한 잎담배중 Phenolic Acid의 분석
Analysis of Phenolic Acids in Tobacco Leaf by GC/MS
초록
A GC/MS method was developed to analyze phenolic acid extract from tobacco leaf. Extracted acids were converted to their methyl esters by refluxing with 3M hydrogen chloride in methanol, and the esters were reacted with his (trimethylsilyl) trifluoroacetamide plus 10% trimethylchlorosilane to silylate the phenolic groups. Derivatives of standard salicylic, p-hydroxybenzoic, vanillic, gentisic, p-coumaric, syringic, ferulic, and sinapic acids prepared by this procedure were analyzed by GC/MS on
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