약학회지 (YAKHAK HOEJI)
- 제18권2호
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- Pages.161-164
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- 1974
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- 0377-9556(pISSN)
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- 2383-9457(eISSN)
m-Hydroxy N-dimethylaniline 유도체의 합성
Synthesis of m-Hydroxy N-dimethylaniline Derivatives
초록
m-Hydroxyaniline was reported to be converted to m-methoxyaniline with dimethylsulfate. However, while repeating the experiment with the same reaction condition, it was learned that the reaction product was not m-methoxyaniline but m-methoxy dimethylaniline. It was confirmed with nmr and ir spectrum and the comparison of bp and mp of the derivatives. Elemental analyses of the derivatives were also consistant with the fact N-dimethylation along with O-methylation occurred.
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