Viscosities of Tetraalkylammonium Chloride Solutions in Isopropanol-Water Mixtures at $30^{\circ}C$

2-프로판올-물 혼합용매중의 tetraalkylammonium chloride 용액의 점도에 관한 연구

  • Byung-Rin Cho (Department of Chemical Engineering, Inha Institute of Technology) ;
  • Young-Ja Lee (Department of Chemical Engineering, Inha Institute of Technology) ;
  • Ikchoon Lee (Department of Applied chemistry, College of Engineering, Seoul National University)
  • 조병린 (인하공과대학 화학공학과) ;
  • 이영자 (인하공과대학 화학공학과) ;
  • 이익춘 (서울대학교 공과대학 응용화학과)
  • Published : 1971.06.30

Abstract

The relative viscosities ${\eta}_r$ of a series of homologous tetraalkylammonium chlorides $Me_4NCl,\;Et_4NCl,\;Pr_4NCl\;and\;Bu_4NCl$ in a series of isopropanol-water mixtures have been determined at $30^{\circ}C$ using Ubbelohde-type viscometers. The viscosity data have been interpreted in terms of viscosity A-and B-coefficients calculated from the Jones-Dole equation, ${\eta}_r=1+AC^{1/2}+BC$. The results indicate that the structure-breaking effect of chloride ion is maximum at 0.l~0.15 mole fraction isopropanol, while the size effect(Einstein effect) of the larger $R_4N^+$ ions is maximum at 0.2~0.25 mole fraction. The results also indicate that in aqueous and water-rich solutions the larger $R_4N^+$ ions (e.g. $Pr_4N+, Bu_4N^+$) appear to be excellent structure-formers and that the viscosities of solutions is not strongly affected by the electrostriction effect of chloride ion.

Keywords

References

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