黃蓍成分에 關한 硏究 (第3報). 有機結晶成分抽出과 結晶確認에 關하여

The Studies on the Components of Astragalus Membranaceus Bunge (Ⅲ) Extraction of the Organic Components with Methanol and Identification of the Crystals

  • 맹기석 (忠南 大學校 工科大學 化工科)
  • Ki Suck Meang (Department of Chemical Engineering, College of Engineering, Chungnam National University)
  • 발행 : 19630900

초록

"Astragalus Membranaceus Bunge", which is a medical herb, grows wild in Manchuria and Korea, is cultivated today in Korea. Any literature about the organic components of "Astragalus Membranaceus Bunge" has been extracted with methanol referring to a literature of "Panax Ginseng C.A. Meyer" and two kinds of colorless crystals were obtained. After recrystallization in absolute alcohol, the melting point has been measured. The one kind was $181-182^{\circ}C$ and the others, $184-186{\circ}C$ respectively. It does not contain nitrogen, sulfur and halogen. By Liebermann's reaction, the one kind was not a carbohydrate but might be a Saponin. Through paper chromatography, taste, melting point, spectrophotometry, and elemental analysis, it was concluded that the other was Sucrose. It has been notified that the compound can be crystallized at the proper temperature, purity, and concentration of the solution and also solvent system.

키워드

참고문헌

  1. 忠南大論文集 v.2 孟琦錫
  2. 서울大學校 敎授 硏究生 硏究報告書 孟琦錫
  3. 韓國植物圖監(下卷草木部) 鄭台鉉
  4. 圖說藥用植物(日本) 西山
  5. 日化誌 v.51 小竹
  6. 藥學雜誌(日本) 近藤;田中
  7. Semimicro 有機定性分析化學 李吉相
  8. 有機化學實驗(日本) 石川;三羽
  9. 파피어크로마토그라피 이길상
  10. 페이퍼크로마토그라프法(日本) 紫田村治
  11. Beckman Instrument Instruction Manual v.305 A