대한화학회지 (Journal of the Korean Chemical Society)

  • 제7권2호
  • /
  • Pages.140-143
  • /
  • 1963
  • /
  • 1017-2548(pISSN)
  • /
  • 2234-8530(eISSN)
대한화학회 (Korean Chemical Society)
권호 표지

${\alpha}$-Athyl-4:6-Diiodo-2:3-Dehydro-2:3:4:6-Tetradeoxy-D-Glucosid 의 合成에 關하여

Studies on the Synthesis of ${\alpha}$-Ethyl-4,6-Diiodo-W,3-Dehydro-2,3,4,6-Tetradeoxy-D-Glucoside

  • 금기창 (忠南大學校 文理科大學 化學科)
  • K. C. Kum (Department of Chemistry, College of Liberal Arts and Sciences, Choong Nam University)
  • 발행 : 19630600
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초록

${\alpha}$-Ethyl-4,6-diiodo-2,3-dehydro-2,3,4,6-tetradeoxy-D-glucoside was synthesized from glucose through a modified Fischer et al. method. The yield of reduction process of an intermediate triacetylglucal, was markedly increased by utilizing lyophilization technique for removing the water in the reaction product.

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참고문헌

  1. Ann. v.110 A.W. Hofman
  2. Ber. v.33 O.Doebner
  3. Ber. v.76 R. Kuhn;D.Jerchel
  4. Ber. v.49 E. Fischer
  5. Ber. v.60 W. Freudenberg
  6. Nature v.165 Korosy
  7. Ber. v.47 E. Fisher
  8. Ann. v.443 M. Bergmann
  9. J. Chem. Soc. v.1950 S. Laland;W.G. Overend;M. Stacey
  10. Ber. v.47 E. Fischer
  11. Ber. v.64 M. Bergmann;W. Freudenberg
  12. Helv. Chem. Acta. v.28 C.A. Grob;D.A. Prins
  13. Ann. v.620 O. Westphal;S. Stirm
  14. J. Am. Chem. Soc. v.51 C.S. Hudson;H.S. Isbell