Synthesis of Cyclohexyl 5-methylbicyclo[2,2,1]hept-2-ene-5-carboxylate

Cyclohexyl 5-methylbicyclo[2,2,1]hept-2-ene-5-carboxylate의 합성

  • Lee, Yoon-Bae (Dept. of Nano Chemical Engineering, Soon Chun Hyang University) ;
  • Ko, You-Jin (Dept. of Nano Chemical Engineering, Soon Chun Hyang University) ;
  • Park, Hee-Kyoung (Dept. of Nano Chemical Engineering, Soon Chun Hyang University)
  • 이윤배 (순천향대학교 나노화학공학과) ;
  • 고유진 (순천향대학교 나노화학공학과) ;
  • 박희경 (순천향대학교 나노화학공학과)
  • Published : 2011.05.27

Abstract

cyclohexyl methacrylate와 cyclopentadiene을 반응하여 cyclohexyl 5-methylbicyclo[2,2,1]hept-2-ene-5-carboxylate를 합성하고 합성된 Norbornene계 화합물을 GC를 이용하여 그 비율을 측정하였고 Column Chromatography를 이용하여 endo와 exo를 분리해 $^1H-NMR$을 이용하여 endo와 exo 화합물의 구조를 확인하였다.

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