Catalyst preparations, coating methods, and supports for micro combustor

초소형 연소기를 위한 촉매 합성, 담지방법 및 담지체

  • 진정근 (KAIST 기계공학과 항공우주공학전공 대학원) ;
  • 김충기 (KAIST 기계공학과 항공우주공학전공 대학원) ;
  • 권세진 (KAIST 기계공학과 항공우주공학전공)
  • Published : 2006.10.20

Abstract

Catalytic combustion is one of the suitable methods for micro power source due to high energy density and no flame quenching. Catalyst loading in the micro structured combustion chamber is one of the most important issues in the development of micro catalytic combustors. In this research, to coat catalyst on the chamber wall, two methods were investigated. First, $Al_2O_3$ was selected as a support of Pt and $Pt/Al_2O_3$ was synthesized through the alumina sol-gel procedure. To improve the coating thickness and adhesion between catalyst and substrate, heat resistant and water solvable organic-inorganic hybrid binder was used. Porous silicon was also investigated as a catalyst support for platinum. Through the parametric studies of current density and etching time, fabrication process of $1{\sim}2{\mu}m$ of diameter and about $25{\mu}m$ depth pores was confirmed. Coated substrates were test in the micro channel combustor which was fabricated by the wet etching and machining of SUS 304. Using $Pt/Al_2O_3$ coated substrate and Pt coated porous silicon substrate, conversion rate of fuel was over 95% for $H_2$/Air premixed gas.

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