Processing of Tin Oxide Nanoparticles by Inert Gas Condensation Method and Characterization

  • Simchi, Abdolreza (Department of Materials Science and Engineering, Sharif University of Technology) ;
  • Kohi, Payam (Institute for Nanoscience and nanotechnology, Sharif University of Technology)
  • Published : 2006.09.24

Abstract

Tin oxide nanoparticles (n-SnO and $n-SnO_2$) were synthesized by the inert gas condensation (IGC) method under dynamic gas flow of oxygen and argon at various conditions. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) method were used to analysis the size, shape and crystal structure of the produced powders. The synthesized particles were mostly amorphous and their size increased with increasing the partial pressure of oxygen in the processing chamber. The particles also became broader in size when higher oxygen pressures were applied. Low temperature annealing at $320^{\circ}C$ in air resulted to crystallization of the amorphous n-SnO particles to $SnO_2$.

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