Applied Chemistry for Engineering (공업화학)
- Volume 30 Issue 5
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- Pages.639-642
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- 2019
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- 1225-0112(pISSN)
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- 2288-4505(eISSN)
DOI QR Code
Synthesis of Hydroxyapatite Using a Cationic Surfactant
양이온성 계면활성제를 이용한 수산화인회석 합성
- Lee, Keunyoung (Department of Chemistry and RINS, Gyeongsang National University) ;
- Kwon, Ki-Young (Department of Chemistry and RINS, Gyeongsang National University)
- Received : 2019.09.09
- Accepted : 2019.09.25
- Published : 2019.10.10
Abstract
Hydroxyapatite (HAP) containing hexadecyltrimethylammonium chloride (CTAC) as a cationic surfactant was prepared by a precipitation method. X-ray diffraction (XRD), transmission electron microscopy (TEM) and micropore physisorption analyzer were used for characterizing the crystal phase, morphology and specific surface area of HAP and CTAC-HAP. After thermal treatment, the specific surface area of both pure HAP and CTAC-HAP were reduced. The sharp rod morphology of CTAC-HAP was changed into a round shape with a smaller aspect ratio after the heat treatment. The morphological change by thermal treatment was also observed in pure HAP. Therefore, the morphological change and decrease of the specific surface area suggested that pores from the removal of CTAC during thermal treatment were not retained.
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Acknowledgement
Supported by : 한국기초과학지원연구원
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