Journal of Magnetics
- Volume 20 Issue 3
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- Pages.221-228
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- 2015
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- 1226-1750(pISSN)
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- 2233-6656(eISSN)
DOI QR Code
Microstructure and Magnetic State of Fe3O4-SiO2 Colloidal Particles
- Kharitonskii, P.V. (Saint Petersburg Electrotechnical University "LETI") ;
- Gareev, K.G. (Saint Petersburg Electrotechnical University "LETI") ;
- Ionin, S.A. (Saint Petersburg Electrotechnical University "LETI") ;
- Ryzhov, V.A. (National Research Centre "Kurchatov Institute") ;
- Bogachev, Yu.V. (Saint Petersburg Electrotechnical University "LETI") ;
- Klimenkov, B.D. (Saint Petersburg Electrotechnical University "LETI") ;
- Kononova, I.E. (Saint Petersburg Electrotechnical University "LETI") ;
- Moshnikov, V.A. (Saint Petersburg Electrotechnical University "LETI")
- Received : 2015.05.02
- Accepted : 2015.08.24
- Published : 2015.09.30
Abstract
Colloidal particles consisted of individual nanosized magnetite grains on the surface of the silica cores were obtained by two-stage sol-gel technique. Size distribution and microstructure of the particles were analyzed using atomic force microscopy, X-ray diffraction and Nitrogen thermal desorption. Magnetic properties of the particles were studied by the method of the longitudinal nonlinear response. It has been shown that nanoparticles of magnetite have a size corresponding to a superparamagnetic state but exhibit hysteresis properties. The phenomenon was explained using the magnetostatic interaction model based on the hypothesis of iron oxide particles cluster aggregation on the silica surface.
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Acknowledgement
Supported by : RFBR
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