Quantitative Analysis of Pentachlorophenol in Paper Products

종이재 중의 Pentachlorophenol 정량 분석

  • Hahn, Airan (Biotechnology & Environment Standards Division, Agency for Technology and Standards) ;
  • Park, Jihye (Biotechnology & Environment Standards Division, Agency for Technology and Standards) ;
  • Choi, Hyeongki (Biotechnology & Environment Standards Division, Agency for Technology and Standards) ;
  • Hong, Sungyeap (Department of Applied Chemistry, Seokyeong University) ;
  • Han, Hyechul (Department of Applied Chemistry, Seokyeong University) ;
  • Jo, Byoungmuk (Department of Paper Science & Engineering, Kangwon National University) ;
  • Oh, Jungsoo (Department of Forest Resources, Dongguk University)
  • 한애란 (기술표준원 생물환경표준과) ;
  • 박지혜 (기술표준원 생물환경표준과) ;
  • 최형기 (기술표준원 생물환경표준과) ;
  • 홍성엽 (서경대학교 화학과) ;
  • 한혜철 (서경대학교 화학과) ;
  • 조병묵 (강원대학교 제지공학과) ;
  • 오정수 (동국대학교 산림자원학과)
  • Received : 2004.07.26
  • Accepted : 2004.12.09
  • Published : 2005.06.10

Abstract

Pentachlorophenol (PCP) is a representative compound of chlorophenol derivatives which are especially toxic and potentially carcinogenic compounds in the priority pollutant list of the EPA (Environmental Protection Agency, USA). The aim of this study was to investigate an analysis method of PCP in infinitesimal quantity retained in paper. PCP in paper was pretreated by solid phase extraction (SPE) in a phenyl cartridge. The extracted sample was acetylated or silylated and analyzed with GC/MS-SIM. The detection sensitivity of silylated PCP was improved significantly when compared with those of PCP itself and acetylated PCP. As a test specimen, an office paper and a wallpaper were used.

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