- Volume 16 Issue 6
Determination of fungicides in wines by solid-phase extraction and gas chromatography with mass selective detection
고체상 추출법과 GC/MS를 이용한 포도주 중의 fungicides 정량
- Park, Gyo-Beom (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology) ;
- Lee, Sueg-Geun (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology)
- Received : 2003.09.15
- Accepted : 2003.09.26
- Published : 2003.12.25
The fungicides, used for grape growth and remained in the wine products from domestic and foreign countries such as vinclozolin, dichlofluanid, penconazole, procymidone were quantitatively analyzed after solid-phase extraction using a GC/MS-SIM method. The results obtained were as follows: for all the samples, the content of procymidone was in the range from 2.2 to
- P. Cabras, A. Angioni, V. L. Garau, F. M. Pirisi, G. A. Farris, G. Madau, G. Emonti, J. Agric. Food Chem., 47, 3854(1999).
- S. Navarro, A. Barba, G. Navarro, N. Vela, J. Oliva, J. Chromatogr., 882, 211(2000).
- A. Prieto, G. Ettiene, D. Mediane, J. Buscema, G. Gonzalez, L. Araujo, Food Addit. Contam. 16, 57( 1999).
- P. Holland, D. McNaughton, C. Malcolm, J. AOAC Int. 77, 79(l994).
- P. Cabras, A. Angioni, V. L. Garau, F. M. Pirisi, V. Brandolini, J. AOAC Int. 81, 1185 (l998).
- G. Nissner, W. Buchberger, R. Eckerstorfer, J. Chromatogr., 846, 341(1999).
- P. Cabras, A. Angioni, J. Agric. Food Chem., 48, 967(2000).
- M. Natangelo, S. Tavazzi, E. benfenati, Anal, Lett, 35, 327(2002).
- J. Wong, M. Webster, C. Halverson, M. Hengel, M. McChesney, K. Ngim, S. Ebeler, presented at the 224th ACS National Meeting, Boston, MA, 2002, abstracts.
- A. Kaufmann, J. AOAC Int. 80, 1302(1997).
- Commission Directive 2oo2/79/EC of 2 October 2002 amending the Annexes to Council Directives 76/895/EEC, 86/362/EEC, 86/363/EEC and 9O/642/EEC as regards the fixing of maximum levels for certain pesticide residues in and on cereals, foodstuffs of animal origin and certain products of plant origin, including fruit and vegetables, European Union, Brussels, 2002.