Amylose Tris(3,5-dimethylphenylcarbamate)-Coated Zirconia as a Chiral Stationary Phase for Micro HPLC

  • Kim, In-Whan ;
  • Okamoto, Yoshio ;
  • Carr, Peter W. ;
  • Ryu, Jong-Kwon ;
  • Park, Jung-Hag
  • Published : 2002.07.20



Chiral stationary phase;Amylose tris(3,5-dimethylphenylcarbamate);Zirconia;HPLC.


  1. Francotte, E. In Chiral Separations: Applications and Technology;Ahuja, S., Ed.; American Chemical Society: Washington, 1997;Chapter 5.
  2. Okamoto, Y.; Kawashima, M.; Yamamoto, K.; Hatada, K. Chem.Lett. 1984, 739.
  3. Okamoto, Y.; Kawashima, M.; Hatada, K. J. Am. Chem. Soc.1984, 106, 5357.
  4. Park, J. H.; Ryu, J. K.; Park, J. K.; McNeff, C. V.; Carr, P. W.Chromatographia 2001, 53, 405.
  5. Ishii, D. In Introduction to Microscale High-Performance LiquidChromatography; Ishii, D., Ed.; VCH: Weinheim, 1988; Chapter 1.
  6. Koller, H.; Rimbock, K. H.; Mannschreck, A. J. Chromatogr. A1983, 282, 89.
  7. Dingenen, J. In A Practical Approach to Chiral Separations byLiquid Chromatography; Subramanian, G., Ed.; VCH: New York,1994; Chapter 6.
  8. Okamoto, O.; Yashima, E. Angew. Chem. Int. Ed. 1998, 37, 1020.<1020::AID-ANIE1020>3.0.CO;2-5
  9. Scott, R. P. W.; Kucera, P. J. Chromatogr. 1976, 125, 251.
  10. Horvath, C. G.; Preiss, B. A.; Lipsky, S. R. Anal. Chem. 1967, 39,1422.
  11. Kirkland, J. J.; van Straten, M. A.; Claessans, H. A. J. Chromatogr.1995, 691, 3.
  12. Jackson, P. T.; Carr, P. W. Chemtech. Oct. 29, 1998.
  13. Okamoto, O.; Kawashima, M.; Hatada, K. J. Chromatogr. 1986,363, 173.
  14. Nawrocki, J.; Dunlap, C. J.; Carr, P. W.; Blackwell, J. A. Biotechnol.Prog. 1994, 10, 561.
  15. Okamoto, Y.; Aburatani, R.; Fukumoto, T.; Hatada, K. Chem. Lett.1987, 1857.
  16. Castells, C. B.; Carr, P. W. Anal. Chem. 1999, 71, 3013.
  17. Okamoto, Y.; Kaida, Y.; Aburatani, R.; Hatada, K. In Chiral Separationsby Liquid Chromatography; Ahuja, S., Ed.; ACS SymposiumSeries 471; American Chemical Society: Washington, DC,1991; pp 101-113.
  18. Park, S. Y.; Park, J. K.; Park, J. H.; McNeff, C. V.; Carr, P. W.Microchem. J. 2001, 70, 179.

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